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Robert Tykot
  • (001) 813 974-7279
  • Professor, Department of Anthropology, University of South Florida Website which includes publications in PDF: http:/... moreedit
Riassunto Si presentano in questa sede i risultati delle analisi non distruttive, effettuate impiegando uno spettrometro portatile in Fluorescenza di raggi X, su circa 180 manufatti preistorici in ossidiana provenienti da 15 siti... more
Riassunto Si presentano in questa sede i risultati delle analisi non distruttive, effettuate impiegando uno spettrometro portatile in Fluorescenza di raggi X, su circa 180 manufatti preistorici in ossidiana provenienti da 15 siti archeologici nell'Orista-nese e nel Cagliaritano in Sardegna, conservati a Roma presso il Museo Prei-storico-Etnografico " Luigi Pigorini ". Congiuntamente alla determinazione fisico-visuale di questi strumenti si esamina l'uso dell'ossidiana nei diversi periodi di tempo e si propongono interpretazioni per modelli cronologici e geografici che possano essere riferiti alla qualità, alla quantità, all'accessibilità e ai fattori socio-economici implicati nell'acquisizione, nella produzione e nell'uso dell'os-sidiana preistorica in Sardegna.

Abstract Results are presented here for the analysis, using a non-destructive portable X-ray fluorescence spectrometer, of nearly 180 prehistoric obsidian artifacts from 15 archaeological sites in the Oristano and Cagliari areas of Sardinia, stored in the Museo Preistorico-Etnografico " Luigi Pigorini " in Rome. Combined with physical/visual assessment of these stone tools, obsidian usage for different time periods is examined, and interpretations proposed for chronological and geographic patterns that may be related to the quality, quantity, access, and socioeconomic factors involved in the acquisition, production, trade, and use of obsidian in prehistoric Sardinia.
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During the Empire, the population of Rome was composed mostly of lower-class free citizens and slaves. Viewed from historical records, the Roman diet included primarily olives, wine, and wheat, but poor and enslaved Romans may have eaten... more
During the Empire, the population of Rome was composed mostly of lower-class free citizens and slaves. Viewed from historical records, the Roman diet included primarily olives, wine, and wheat, but poor and enslaved Romans may have eaten whatever they were able to find and afford, leading to significant heterogeneity in the Roman diet. Previous carbon and nitrogen isotope analyses of skeletons from Imperial Italy have begun to reveal variation in diet, but little is known about what people ate in the capital city. This study complements previous work by adding new isotope data from human skeletons found in two Imperial-period (1st–3rd centuries AD) cemeteries in Rome. These data suggest that urban and suburban diets differed, most notably in the consumption of the C4 grain millet. Comparing these new data with all published palaeodietary data from Imperial Italy demonstrates that significant variation existed in the diet of the common people.► We performed C and N isotope analyses on 48 individuals from Imperial Rome. ► Most people consumed a diet composed of C3 plants and aquatic protein. ► One adult had a predominantly C4 diet, and one child had not been fully weaned. ► People living in the suburbs ate more C4 resources than people living near the city. ► Comparison with other data from Imperial Italy suggests heterogeneity in the diet.
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In this paper we test the hypothesis that an intensification of maize production preceded the development of a regional Moche political economy in the Moche Valley of north coastal Peru during the Early Intermediate period (400 B.C.-A.D.... more
In this paper we test the hypothesis that an intensification of maize production preceded the development of a regional Moche political economy in the Moche Valley of north coastal Peru during the Early Intermediate period (400 B.C.-A.D. 600). To do so we analyze stable isotopic signatures of 48 bone apatite and 17 tooth enamel samples from human remains recovered from the site of Cerro Oreja, a large urban and ceremonial center in the Moche Valley. These remains date to the Guañape, Salinar, or Gallinazo phases and provide a diachronic picture of subsistence before the appearance of the Southern Moche state. The most notable patterns identified in the study include a lack of significant change in δ13Capatite values from the Guañape to Salinar phases, followed by a significant enrichment in δ13Capatite values from the Salinar to Gallinazo phases. Several lines of evidence, including archaeological context, dental data, and comparative carbon stable isotope data from experimental animal studies and studies of archaeological human remains support the interpretation that the observed 13C enrichment in stable isotope values in the Gallinazo phase primarily reflects maize intensification. The stable isotope data from Cerro Oreja thus suggest that a shift in subsistence toward a highly productive and storable crop may have served as an important precursor to state development during the Early Intermediate period in the Moche Valley.
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Use of inductively coupled plasma-mass spectrometry (ICPMS) coupled to a laser-ablation sample introduction system (LA-ICP-MS) as a minimally destructive method for chemical characterization of archaeological materials has gained favor... more
Use of inductively coupled plasma-mass spectrometry (ICPMS) coupled to a laser-ablation sample introduction system (LA-ICP-MS) as a minimally destructive method for chemical characterization of archaeological materials has gained favor during the past few years. Although still a relatively new analytical tectmique in archaeology, LA-ICP-MS has been demonstrated to be a productive avenue of research for chemical characterization of obsidian, chert, pottery, painted and glazed surfaces, and human bone and teeth. Archaeological applications of LA-ICP-MS and comparisons with other analytical methods are described.
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ABSTRACT This volume reprints 20 chapters from the editors’ comprehensive Histories of Maize (2006) that are relevant to Mesoamerican specialists and students. New findings and interpretations from the past three years have been... more
ABSTRACT This volume reprints 20 chapters from the editors’ comprehensive Histories of Maize (2006) that are relevant to Mesoamerican specialists and students. New findings and interpretations from the past three years have been included. Histories of Maize is the most comprehensive reference source on the botanical, genetic, archaeological, and anthropological aspects of ancient maize published. Included in this abridged volume are new introductory and concluding chapters and updated material on isotopic research. State of the art research on maize chronology, molecular biology, and stable carbon isotope research on ancient human diets have provided additional lines of evidence on the changing role of maize through time and space and its spread throughout the Americas. The multidisciplinary evidence from the social and biological sciences presented in this volume have generated a much more complex picture of the economic, political, and religious significance of maize.
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In the Neolithic and Copper Age collective burials of the Portuguese Estremadura, the majority of material culture and skeletal remains are highly commingled, making it difficult for archaeologists to evaluate social status by linking... more
In the Neolithic and Copper Age collective burials of the Portuguese Estremadura, the majority of material culture and skeletal remains are highly commingled, making it difficult for archaeologists to evaluate social status by linking individuals with specific grave goods. In these circumstances, bio-anthropological data about individual life histories offer an additional avenue of investigation into social complexity among prehistoric communities practising collective burial. In this study, stable isotope data were gathered from 81 individuals from seven collective burial sites and one settlement, the fortified site of Zambujal, in order to determine if significant dietary differences exist within or between burials that may point to patterns of social differentiation, both at individual sites and across the region. While in general all of the sampled individuals consumed fairly homogeneous diets based on terrestrial animal proteins and C3 plants, this study found that statistically significant differences in δ13Cap and δ15N values exist between several sites, which may indicate socially differentiated consumption of meat and plants. Additionally, statistically significant differences were found in δ15N values between adults and juveniles, which may either be attributable to protein-restrictive child-feeding practices or physiological processes related to skeletal growth and development.
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ABSTRACT Obsidian artifacts have been found at many prehistoric sites in Sicily, yet only a few studies have been done to determine the specific geological sources and subsources used. In 2012, nearly 600 artifacts from 25 archaeological... more
ABSTRACT Obsidian artifacts have been found at many prehistoric sites in Sicily, yet only a few studies have been done to determine the specific geological sources and subsources used. In 2012, nearly 600 artifacts from 25 archaeological sites dating from the Neolithic, Copper, and Bronze Ages (ca. 6th-2nd millennia BC) were analyzed non-destructively using a hand-held portable X-ray fluorescence spectrometer, in museums that would not allow removal of the artifacts. In addition, all of the artifacts were techno-typologically analyzed to understand how obsidian was reduced and used through time. A Bruker III-SD was used to produce data for trace elements Rb, Sr, Y, Zr, and Nb which were calibrated against international obsidian standards, and compared with results obtained with the same instrument on geological sources and subsources in the Mediterranean region. All artifacts tested came either from Lipari or Pantelleria, confirming visually-based predictions but also demonstrating that multiple geological subsources were used on each island. The majority of the obsidian artifacts were blades, while a small percentage were cores. These results are used to assess variation based on site location, time period, and lithic typology, and to inform us about contact, exchange, and socioeconomic aspects of the ancient societies involved and if they changed over time.
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ABSTRACT The Central Mediterranean islands of Lipari, Palmarola, Pantelleria, and Sardinia are known to be the only sources of obsidian in that region (Tykot, 2002). The obsidian on each source island has a unique chemical composition... more
ABSTRACT The Central Mediterranean islands of Lipari, Palmarola, Pantelleria, and Sardinia are known to be the only sources of obsidian in that region (Tykot, 2002). The obsidian on each source island has a unique chemical composition (i.e., a fingerprint) that has allowed Tykot (2002) to provenance Neolithic obsidian artifacts from archaeological sites throughout the Central Mediterranean to these four sources. Thus, Tykot (2002) revealed material distribution patterns otherwise inaccessible to archaeologists. An exploratory study by McDougall et al. (1983) demonstrated the potential use of magnetic properties to distinguish Central Mediterranean obsidians. If each obsidian source group has a unique magnetic fingerprint, magnetic provenancing might serve as a quick, inexpensive, and non-destructive alternative to chemical provenancing. Our research continues the work started by McDougall et al.; we set out to characterize the Central Mediterranean obsidians and search for magnetic fingerprints that distinguish them. Our preliminary study of the magnetic properties of 30 geologic obsidian specimens from Sardinia A, B, and C subgroups and the three other Central Mediterranean island sources suggests that each source has a unique combination of magnetic properties that could allow magnetic provenancing of archaeological obsidians. For example, the combination of natural remanent magnetization (NRM; median [med] = 2.46 x 10-4 Am2/kg, interquartile range [IQR] = 9.77 x 10-4 Am2/kg) and magnetic susceptibility (low field, low frequency magnetic susceptibility [chilflf]: med = 27.0 x 10-6 m3/kg, IQR = 75.9 x 10-6 m3/kg) seems to have good potential to discriminate the groups. However, statistical analysis shows that there is significant overlap in the confidence intervals of these variables, a limitation which appears to be partially imposed at this point by the small sample size. Discriminant analysis of several magnetic variables also shows potential to assist in classification (i.e., provenancing) of Central Mediterranean obsidians. We have obtained discriminant functions that correctly classify over 80% of the obsidian specimens in leave-one-out cross validations using as few as three log- transformed magnetic parameters: NRM, chilflf, and saturation isothermal remanent magnetization (SIRM; med = 7.59 x 10-3 Am2/kg, IQR = 2.85 x 10-2 Am2/kg). Backfield coercivity of remanence, median destructive field, percent frequency effect, and saturation coercivity seem to contribute the least to group discrimination, yet their effects are statistically significant. Even though initial tests of discriminant analysis look promising, it should be noted that the small sample sizes and relatively large number of variables used in the discriminant analyses violate the test's assumptions and may make the resulting discriminant functions unusable; this will be addressed in future research. The results from our preliminary study suggest that the Central Mediterranean sources of obsidian might have characteristic and distinguishable magnetic fingerprints. However, many more geologic obsidian specimens must be measured to define the ranges of the source groups' magnetic properties and to further test this hypothesis.
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Se presenta nueva información sobre análisis de isótopos estables en esmalte, colágeno y apatita de restos humanos arqueológicos de la costa centro-septentrional de Patagonia y el valle inferior del río Chubut. La muestra cubre un rango... more
Se presenta nueva información sobre análisis de isótopos estables en esmalte, colágeno y apatita de restos humanos arqueológicos de la costa centro-septentrional de Patagonia y el valle inferior del río Chubut. La muestra cubre un rango temporal de entre 6000 y 200 años AP. Los resultados se discuten en función del registro arqueofaunístico y de una base de datos sobre la ecología isotópica del área. Se evalúa la variabilidad temporal y espacial y se discute el papel de los recursos marinos en la dieta y la movilidad.
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Background Each year during the Roman Empire (c. 1st-4th centuries AD), millions of immigrants arrived at Rome, most of them slaves. The general diet of people in the city consisted primarily of grain, olives, and wine, but historical... more
Background Each year during the Roman Empire (c. 1st-4th centuries AD), millions of immigrants arrived at Rome, most of them slaves. The general diet of people in the city consisted primarily of grain, olives, and wine, but historical sources indicate that dietary practices varied based on age, sex, and social class (Garnsey 1999, Purcell 2003, Wilkins & Hill 2006). Recent palaeodietary studies of populations in the Roman countryside also demonstrate marked differences in diet in the Imperial period (Prowse 2001, Prowse et al. ...
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... In Archaeological Chemistry; Orna, M.; ACS Symposium Series; American Chemical Society: Washington, DC, 1996. Page 2. 10. ... In Archaeological Chemistry; Orna, M.; ACS Symposium Series; American Chemical Society: Washington, DC,... more
... In Archaeological Chemistry; Orna, M.; ACS Symposium Series; American Chemical Society: Washington, DC, 1996. Page 2. 10. ... In Archaeological Chemistry; Orna, M.; ACS Symposium Series; American Chemical Society: Washington, DC, 1996. Page 3. 118 ...
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Elemental analysis is a fundamental method of analysis on archaeological materials to address their overall composition or identify the source of their geological components, yet having access to instrumentation, its often destructive... more
Elemental analysis is a fundamental method of analysis on archaeological materials to address their overall composition or identify the source of their geological components, yet having access to instrumentation, its often destructive nature, and the time and cost of analyses have limited the number and/or size of archaeological artifacts tested. The development of portable X-ray fluorescence (pXRF) instruments over the past decade, however, has allowed nondestructive analyses to be conducted in museums around the world, on virtually any size artifact, producing data for up to several hundred samples per day. Major issues have been raised, however, about the sensitivity, precision, and accuracy of these devices, and the limitation of performing surface analysis on potentially heterogeneous objects. The advantages and limitations of pXRF are discussed here regarding archaeological studies of obsidian, ceramics, metals, bone, and painted materials.
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The study of bi-phase (i.e. matrix and clasts) geochemical composition of ceramic artifacts is a very powerful tool in fingerprinting the raw materials used by ancient manufacturers (clay sources, tempering materials, coloring agents,... more
The study of bi-phase (i.e. matrix and clasts) geochemical composition of ceramic artifacts is a very powerful tool in fingerprinting the raw materials used by ancient manufacturers (clay sources, tempering materials, coloring agents, etc.), as well as in understanding the physical parameters of the manufacturing techniques. Reliable datasets often require the deployment of destructive techniques that will irremediably damage the artifact. Recent advances in portable X-ray fluorescence instrumentation (pXRF) allow for quick measurements of a range of chemical elements that not too long ago were available only through complicated and often destructive means of analytical chemistry (instrumental neutron activation analysis - INAA, inductively coupled plasma mass spectrometry - ICP-MS, direct coupled plasma-optical emission spectroscopy - DCP-OES etc.). In this contribution we present a comparison of datasets acquired by means of pXRF, DCP-OES, and ICP-MS on Bronze Age ceramics from Fa...
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Presented here are results from the non-destructive portable X-ray fluorescence (pXRF) analysis of ceramic artifacts in Italy, Malta, and Croatia, dating to the Neolithic, Chalcolithic, Bronze, and Iron Ages, with a focus on the... more
Presented here are results from the non-destructive portable X-ray fluorescence (pXRF) analysis of ceramic artifacts in Italy, Malta, and Croatia, dating to the Neolithic, Chalcolithic, Bronze, and Iron Ages, with a focus on the advantages and limitations of this method of analysis in identifying local vs. non-local pottery, and their “history” of mobility and socioeconomic significance. While providing opportunities for conducting analytical research in museums and other places where borrowing or sampling the artifacts is not permitted, pXRF users must be aware of its limitations, including detection limits, which elements can be measured, potential heterogeneity of the material being tested, and comparison with analytical data from other studies. Unlike obsidian, for which all Mediterranean sources can be distinguished, there are limitations in the use of pXRF on ceramics when compared with regular XRF, INAA, and LA-ICP-MS. Most of this is the detection limits of the pXRF, so that...
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A systematic, large-scale analytical program for obsidian from prehistoric archaeological sites in Sicily was conducted in 2012 and 2013. With the permission of several museums and superintendencies, over 1500 obsidian artifacts from 30... more
A systematic, large-scale analytical program for obsidian from prehistoric archaeological sites in Sicily was conducted in 2012 and 2013. With the permission of several museums and superintendencies, over 1500 obsidian artifacts from 30 sites dating from the Early Neolithic to the Bronze Age were examined and characterized by their typology and technological features, and analyzed non-destructively using a Bruker III-SD portable X-ray fluorescence spectrometer to determine their specific geological source and reconstruct transport/trade routes. This instrument has been shown to distinguish all island sources in the Mediterranean, and the subsources on each, including Gabellotto and Canneto Dentro on Lipari, and Balata dei Turchi and Lago di Venere on Pantelleria. Most previous studies of obsidian in Sicily only used visual characteristics to distinguish Lipari from Pantelleria, with chemical analyses limited to Grotta dell’Uzzo, the Milena territory, and Ustica. In this study, analy...
By the Late Bronze Age in Sicily and the Mediterranean, long distance exchange was well established as shown by materials such as copper oxhide ingots, amber, glass, ivory, and both decorated pottery and ceramic transport vessels. At some... more
By the Late Bronze Age in Sicily and the Mediterranean, long distance exchange was well established as shown by materials such as copper oxhide ingots, amber, glass, ivory, and both decorated pottery and ceramic transport vessels. At some sites in southeastern Sicily, the large quantity of Mycenaean-style ceramics suggests the existence of established commercial routes with the Aegean. Similarly, Maltese-style ceramics have also been found in this region. Regular maritime connections were an important feature of the Bronze Age central Mediterranean. In this study, non-destructive elemental analysis was performed on ceramics from both the Museo Archeologico Regionale Paolo Orsi in Siracusa and the Museo Civico in Milena. Specifically, a portable Bruker III-SD X-ray fluorescence spectrometer (pXRF) was used with filter, voltage and amperage settings chosen to enhance results for trace elements Rb, Sr, Y, Zr, and Nb, as well as major elements including Fe. Multiple spot analyses, for 1...

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The Site of Cucuruzzu The casteddu (stone enclosure) of Cucuruzzu, Corsica, constitutes one of the most remarkable places of the Corsican Bronze Age (Figure 1). Roger Grosjean directed several excavations there throughout the 1960s, and... more
The Site of Cucuruzzu The casteddu (stone enclosure) of Cucuruzzu, Corsica, constitutes one of the most remarkable places of the Corsican Bronze Age (Figure 1). Roger Grosjean directed several excavations there throughout the 1960s, and François de Lanfranchi continued to explore the site in the 1970s. The built environment consists of a wide stone enclosure girding the stone tower located at the most prominent point of the location. The geographic situation of the complex and its architecture are consistent with a defensive function. However, the presence of sherds of large storing jars and of unfired clay coils in the three chambers located within the thickness of the enclosure walls suggests that the site may also have played a political role as a manufacturing and redistribution center at a regional level. In the summer 2015, a preventive excavation took place in two different locations of the enclosure in prevision of a series of planned interventions aimed at ensuring the safety of the visitors. The ceramic material found at this occasion in the stratigraphic unit 105 of the sector 1 was identified as typical of the ceramic production of the beginning of the Final Bronze Age (1200-950 BC), an attribution that was later confirmed by radiocarbon dating (1300-1075 cal BC, 95%). Method This study includes 67 sherds and a daub fragment found during the 2015 excavation, as well as a clay sample from a deposit located in the vicinity of the site (Figure 3). A portable Bruker III-SD X-ray fluorescence (pXRF) spectrometer was used to determine the value six trace elements that known for being indicative of the geological origin of the clay: rubidium, strontium, yttrium, zirconium, niobium, and thorium (Tykot 2016). In order to make sure no slip or painting interfered with the measurement, each sherd was analyzed twice: once on the inner surface and once on the outer surface. The average of the two values was retained for subsequent statistical analyses. The samples were then classified into different chemical groups through cluster analysis, principal component analysis, and discriminant analysis. Final Bronze Age Ceramics in Corsica A genuine rupture occurred in the field of ceramic production at the beginning of the Final Bronze Age in southern Corsica. In effect, this period corresponds to the appearance of a new ceramic assemblage, designated as the " ACC " assemblage in reference to the sites (Apazzu, Cuccuruzzu, and Castidetta) where it was first identified (Peche-Quilichini 2014). ACC assemblages consist of a coarseware, reminiscent of earlier productions, and of a fineware that has no antecedent in the region. The manufacturing operational sequence of the fineware include practices such as surface burnishing and firing in a reducing atmosphere, which may point at a specialized rather than domestic production (Figure 2). Since several authors also place the appearance of the casteddi at the beginning of the Final Bronze Age, there is a possibility that the two phenomena may have been related. In particular, if the ACC fineware was indeed made by specialists, one would expect its production to take place in the casteddi, where it could presumably be controlled by the local elite. The aim of this study is to explore the production and the distribution of ACC ceramics through the analysis of the chemical composition of the paste of the vessels. References Peche-Quilichini, Kewin 2014 Protohistoire d'une île Vaisselles céramiques du Bronze final et du premier âge du Fer de Corse (1200-550 av. J.-C.).
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